About 300 people are feared dead after a dam collapsed at an iron ore mine in south-eastern Brazil, officials say.
The break caused a sea of muddy sludge that buried the dam’s cafeteria where workers were eating lunch on Friday.
Rescue teams used earth-moving machinery at the site near the town of Brumadinho, in Minas Gerais state.
State governor Romeu Zema said there was little chance of finding people alive. So far nine people have been confirmed dead.
It is not clear what caused the collapse of the dam, owned by Brazil’s largest mining company, Vale.
On Saturday, state prosecutors filed a request to freeze 5bn reais ($1.33bn; £1bn) on Vale’s accounts to help fund recovery works and handle damage claims.
The collapse comes just over three years since a dam burst in Mariana, also in Minas Gerais, killing 19 people, in what is considered Brazil’s worst environmental disaster.
The dam near Feijão iron ore mine burst its barrier at around 13:00 local time (15:00 GMT) on Friday, flooding another dam down below.
The torrent of sludge cut through the dam’s complex, nearby farms and the neighbourhood where many of the workers live, destroying houses and vehicles.
There are reports that the dam’s alarm system – which local residents had been trained to respond to – failed at the time of the accident.
But Vale president Fabio Schvartsman said the accident may have occurred too quickly for a siren which triggers security protocols to be activated.
The Globo website later reported that rescue officials provided the following breakdown on the number of the missing:
Dozens of trapped people, many of them covered in mud, had to be evacuated by helicopter as roads were destroyed.
Many other residents have been evacuated as a safety measure.
The company’s chief executive Fabio Schvartsman said only one-third of the roughly 300 workers at the site had been accounted for.
Local firefighters also said the number of missing in the area could be as many as 300.
“I’m anxious, I want news,” 28-year-old Helton Pereira told the BBC as he waited outside a hospital in nearby Belo Horizonte – his 28-year-old wife and 35-year-old sister worked at the dam’s cafeteria and were both missing.
The search is being carried out by 100 firefighters with 100 more expected to join them on Saturday.
“From now, the odds are minimal and it’s most likely we’ll recover only bodies,” Governor Zema said.
Built in 1976, the dam was one of several in the area and it was used to hold residue from the mine.
It had capacity for 12m cubic metres and had been an inactive site for three years, Vale said.
